苹果农药残留检测方法研究进展

doi:10.12190/j.issn.2096-1197.2022.06.11

Abstract

Abstract:

Apple pesticide residues not only compromise food safety，but also seriously endanger public health. Accurate and rapid detection of pesticide residues is an important means to ensure food safety. This paper reviewed the detection methods of pesticide residues in apple in recent years and introduced traditional detection techniques such as gas chromatography，gas chromatography-mass spectrometry，high performance liquid chromatography，and high performance liquid chromatography-mass spectrometry，as well as rapid detection techniques including surface enhanced Raman spectroscopy，near infrared spectroscopy，electrochemical method，and several new detectable techniques in the application of pesticide residues detection in apple. Also it look forward to the combination of traditional detection techniques and rapid detection techniques to solve the problem in order to provide technical support for the detection of pesticide residues in apple.

Key words: Apple, Pesticide residues, Detection method

CLC Number:

S661.1

WU Zhenting, LIU Xuefeng, LIANG Hairong, WANG Chunying, NIU Xiaoxiao, YANG Mo. Research progress in detection methods of pesticide residues in apple[J].Journal of Northern Agriculture, 2022, 50(6): 80-87.

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URL: https://journal30.magtechjournal.com/bfnyxb/EN/10.12190/j.issn.2096-1197.2022.06.11

https://journal30.magtechjournal.com/bfnyxb/EN/Y2022/V50/I6/80

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References 58

[1]	高小松, 胡晓望, 张新社. 苹果农药残留产生的原因及对策[J]. 北京农业, 2013(18):217.
[2]	PARK B K, KWON S H, YEOM M S, et al. Detection of pesticide residues and risk assessment from the local fruits and vegetables in Incheon,Korea[J]. Scientific Reports, 2022, 12(1):9613. doi: 10.1038/s41598-022-13576-5
[3]	杨宸. 改进QuEChERS技术结合GC-MS/MS测定苹果和梨中的农药多残留[D]. 泰安: 山东农业大学, 2019.
[4]	张贤霞. 陕西苹果农药使用现状调查及相关杀虫剂残留测定[D]. 咸阳: 西北农林科技大学, 2018.
[5]	AFIFY A S, ABDALLAH M, ISMAIL S A, et al. Development of GC-MS/MS method for environmental monitoring of 49 pesticide residues in food commodities in Al-Rass,Al-Qassim region,Saudi Arabia[J]. Arabian Journal of Chemistry, 2022, 15(11):104199. doi: 10.1016/j.arabjc.2022.104199
[6]	霍剑威. 智能数据库建立三重四极杆气质方法对多农药残留进行快速筛查的应用研究[D]. 广州: 华南理工大学, 2019.
[7]	赵航. 固态SERS基底的制备及其检测水果表面农药残留的研究[D]. 哈尔滨: 哈尔滨工业大学, 2019.
[8]	SOUZA TETTE P A, ROCHA GUIDI L, DE ABREU GLÓRIA M B, et al. Pesticides in honey:A review on chromatographic analytical methods[J]. Talanta, 2016, 149:124-141. doi: 10.1016/j.talanta.2015.11.045
[9]	袁景. 基于表面增强拉曼光谱的真菌毒素和农药残留的检测及其应用[D]. 上海: 上海师范大学, 2016.
[10]	BEMPAH C K, DONKOR A, YEBOAH P O, et al. A preliminary assessment of consumer′s exposure to organochlorine pesticides in fruits and vegetables and the potential health risk in Accra Metropolis,Ghana[J]. Food Chemistry, 2011, 128(4):1058-1065. doi: 10.1016/j.foodchem.2011.04.013
[11]	周璐. 油点萃取—气相色谱/质谱法测定苹果汁中的有机磷农药残留[D]. 泰安: 山东农业大学, 2012.
[12]	ABDEL-KADER Z M. Determination of carotenoids in foods by high-performance liquid chromatography[J]. Die Nahrung, 1991, 35(7):689-693. doi: 10.1002/(ISSN)1521-3803
[13]	CAMPILLO, PEÑALVER, HERNÁNDEZ-CÓRDOBA. A sensitive solid-phase microextraction/gas chromatography-based procedure for determining pentachlorophenol in food[J]. Food Additives & Contaminants, 2007, 24(7):777-783.
[14]	OKIHASHI M, AKUTSU K, OBANA H, et al. Determination of triazine herbicides in foods with liquid chromatography mass spectrometry[J]. The Analyst, 2000, 125(11):1966-1969. doi: 10.1039/b007155m
[15]	FAUGHNAN K T, WOODRUFF M A. Modified gas chromatographic/mass spectrometric method for determination of daminozide in high protein food products[J]. Journal of AOAC International, 1991, 74(4):682-692. doi: 10.1093/jaoac/74.4.682
[16]	杨明, 涂凤琴, 伊鋆, 等. 蔬菜中农药残留分析检测技术的研究进展[J]. 河南工业大学学报(自然科学版), 2020, 41(6):119-128.
[17]	易军. 食品中农药残留分析技术的研究与应用[D]. 厦门: 厦门大学, 2002.
[18]	杭广林. 基质固相分散-气相色谱法测定苹果中的多种农药残留[J]. 河南农业, 2021(35):52-53.
[19]	刘大鹏, 王秋月, 孙晓仲. QuEChERS/气相色谱法测定苹果中有机磷农药残留研究[J]. 食品安全导刊, 2018(21):134.
[20]	石亚亭, 谢明杰, 常建中, 等. QuECHERS-GC-FPD法测定蔬菜水果中的12种有机磷农药残留[J]. 广州化学, 2021, 46(3):83-88.
[21]	陈姣姣. 高效氯氟氰菊酯、呋虫胺及其代谢产物在苹果上的残留检测及消解动态研究[D]. 贵阳: 贵州大学, 2017.
[22]	黄玉婷. 分散液液微萃取技术及其在24种农药残留分析中的应用研究[D]. 北京: 中国农业科学院, 2013.
[23]	高青珍, 刘肃. QuEChERS-悬浮固化分散液液微萃取气相色谱法测定苹果、柑橘中7种有机磷农药[J]. 农产品质量与安全, 2016(5):59-63.
[24]	万郑凯, 何娟, 康长安, 等. 气相色谱-质谱联用在农药残留检测方面的应用进展[J]. 分析测试技术与仪器, 2006, 12(1):51-58.
[25]	王小琴, 王璐, 王庆国, 等. 气相色谱-质谱联用测定苹果中7种有机磷农药残留[J]. 食品安全导刊, 2021(32):110-112.
[26]	李军. 苹果中拟除虫菊酯类农药残留测定方法的研究[J]. 山东农业科学, 2013, 45(12):87-90.
[27]	蔡理胜, 沈伟健, 王正萍, 等. 气相色谱-电子轰击电离/正化学电离质谱法测定白菜和苹果中3种有机锡类农药残留[J]. 色谱, 2017, 35(11):1177-1183. doi: 10.3724/SP.J.1123.2017.07011
[28]	虞游毅, 杨璐, 廖享, 等. 固相微萃取-气相色谱质谱联用法测定苹果中4种有机氯类农药残留[J]. 农药, 2018, 57(1):54-57.
[29]	ANASTASSIADES M, LEHOTAY S J, ŠTAJNBAHER D, et al. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce[J]. Journal of AOAC International, 2003, 86(2):412-431. doi: 10.1093/jaoac/86.2.412
[30]	李梓彤, 李浩浩, 杨海旭, 等. QuEChERS-气相色谱串联质谱法测定苹果中丙环唑农药残留及基质效应研究[J]. 食品安全导刊, 2022(9):117-119.
[31]	高霞, 陈辉, 谭敏, 等. QuEChERS-气相色谱质谱法测定苹果中45种农药残留[J]. 食品工业科技, 2020, 41(16):243-251.
[32]	刘涛. 水果表面农药残留快速检测方法及模型研究[D]. 南昌: 华东交通大学, 2011.
[33]	王其昌. 高速液相色谱法及其仪器[J]. 分析仪器, 1976(4):1-60.
[34]	张慧荣, 周围, 王波, 等. UPLC法测定苹果中4种新型植物生长调节剂农药残留[J]. 分析试验室, 2014, 33(9):1097-1100.
[35]	李涛, 邵林, 杨丽芬, 等. QuEChERS-高效液相色谱法同时测定苹果中7种苯甲酰脲类农药残留[J]. 食品安全质量检测学报, 2020, 11(20):7591-7597.
[36]	彭帆, 谭雨嫣, 张珊珊, 等. 离子液体分散液液微萃取-高效液相色谱分析苹果中有机磷农药残留[J]. 湖北大学学报(自然科学版), 2021, 43(2):109-115.
[37]	甘宾宾, 汤艳荣, 蒋世琼. 高效液相色谱-质谱联用技术在食品安全中的应用及进展[J]. 化工技术与开发, 2009, 38(12):33-37.
[38]	何成军, 成长玉, 钟慈平, 等. QuEChERS-UPLC-MS/MS法快速测定苹果中304种农药残留[J]. 食品工业, 2022, 43(9):305-310.
[39]	陈汝, 王金政, 王贵平, 等. QuEChERS-UPLC-MS/MS法检测苹果中5种农药残留[J]. 分析试验室, 2021, 40(2):163-168.
[40]	付尧, 韦文芳, 刘冬梅, 等. 苯菌灵在苹果上的残留分布研究[J]. 农业灾害研究, 2020, 10(3):181-184.
[41]	韩煜晖, 张爱英, 梅寒. 超高效液相色谱-串联质谱法测定苹果中辛硫磷残留[J]. 安徽农学通报, 2019, 25(23):111-113.
[42]	张子阳, 黄丹丹, 徐志伟, 等. 固相萃取-超高效液相色谱-串联质谱法测定苹果中10种农药残留[J]. 化学研究与应用, 2019, 31(11):1985-1990.
[43]	HART R M, BERGMAN J G, WOKAUN A. Surface-enhanced Raman scattering from silver particles on polymer-replica substrates[J]. Optics Letters, 1982, 7(3):105-107. pmid: 19710838
[44]	董涛. 基于表面增强拉曼光谱的土壤农残快速检测方法研究[D]. 杭州: 浙江大学, 2019.
[45]	彭彦昆, 田文健, 郭庆辉, 等. 基于增强拉曼光谱的苹果中啶虫脒农药残留的无损定量分析[J]. 农业工程学报, 2021, 37(14):310-316.
[46]	叶露. 基于表面增强拉曼光谱技术的蔬菜水果中百草枯的快速检测方法研究[D]. 扬州: 扬州大学, 2021.
[47]	张旭, 陈阳, 严霞, 等. 基于SERS技术的果蔬表皮农药残留快速检测方法研究[J]. 中国海洋大学学报(自然科学版), 2021, 51(2):127-134.
[48]	刘雨平. 基于SERS检定水果表面农药残留水平的关键技术研究[D]. 哈尔滨: 哈尔滨工业大学, 2019.
[49]	黄智斌. 基于Au@Ag纳米棒的2D基底的制备及其用于表面增强拉曼检测苹果中的福美双[D]. 广州: 华南理工大学, 2020.
[50]	邵菲. 静电纺丝制备柔性表面增强拉曼散射基底及其对农药残留快速检测[D]. 上海: 上海师范大学, 2020.
[51]	吕赫一. 基于近红外光谱的苹果品质快速无损检测方法研究[D]. 哈尔滨: 哈尔滨理工大学, 2021.
[52]	陈淑一, 赵全明, 董大明. 对比主成分分析的近红外光谱测量及其在水果农药残留识别中的应用[J]. 光谱学与光谱分析, 2020, 40(3):917-921.
[53]	张晓, 蒋霞, 石鲁珍, 等. 基于GA的偏最小二乘法在近红外光谱识别苹果表面农药残留量的应用[J]. 科技通报, 2019, 35(8):28-33.
[54]	常玉琪. 基于碳基纳米复合物电化学传感器的农药残留快速检测应用研究[D]. 新乡: 河南科技学院, 2022.
[55]	唐文志. 有机磷农药和硝酸盐的电化学快速检测方法研究[D]. 杭州: 浙江大学, 2016.
[56]	乔琦. 基于高光谱-电子鼻的苹果农残自动化检测研究[D]. 吉林: 东北电力大学, 2021.
[57]	杨曼青, 陆桥, ZENOBI R, 等. 激光解吸介质阻挡放电电离质谱快速检测苹果表皮的农药残留[J]. 厦门大学学报(自然科学版), 2022, 61(1):18-24.
[58]	赵贤德, 董大明, 矫雷子, 等. 纳米增强激光诱导击穿光谱的苹果表面农药残留检测[J]. 光谱学与光谱分析, 2019, 39(7):2210-2216.

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